· Start Dyeing @50°C; ensure the starting bath pH be 6; adjust with Acetic Acid if necessary.
· Add salt (vacuum or Glauber’s salt) and hold for 15 minutes
· Add ½ the volume of dissolved and filtered dyestuff and hold 10 minutes.
· Add ½ the volume of dissolved and filtered dyestuff and hold 10 minutes.
· Raise the temperature @2°C/minute to 80°C and hold for 20 minutes.
· Add ½ alkali (Soda ash) and hold 25 minutes.
· Add ½ alkali (Soda ash) and hold for 30 minutes.
· Check sample
· Drain
· Cold wash (10 + 10 minutes)
· Neutralize @ 40°C with adequate qty of Acetic acid.
· Cold wash – 10 minutes
· Hot Wash @ 70°C (2°C/minute) – 10 minutes
· Soap @ 95°C – 15 minutes (1st soap)
· Soap @ 95°C – 15 minutes (2nd soap)
· Soap @ 95°C – 15 minutes (3rd soap)
· Hot Wash
· Sample check for shade and wash fastness
· Cold wash (10 + 10) minutes
· Acid wash with 1 gpl of acetic acid
· In the same acid bath – cationic softener treatment – 20 minutes
· Check pH – 6
· Unload.